Apparatus for preparing hydrazo-dicarbonamide using urea as...

Chemical apparatus and process disinfecting – deodorizing – preser – Chemical reactor – With means applying electromagnetic wave energy or...

Reexamination Certificate

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C422S187000, C564S034000

Reexamination Certificate

active

07422727

ABSTRACT:
The present invention relates to a method and apparatus for preparing hydrazodicarbonamide using urea as starting material economically and environmentally desirably. The apparatus includes a pyrolysis furnace to obtain biuret and ammonia by pyrolyzing urea; a recrystallization reactor to purify the biuret obtained from the pyrolysis furnace; a first reactor to obtain an metal monohalobiuret salt by reacting the biuret with metal hypohalogen compound or with halogen and base; a second reactor to synthesize the hydrazodicarbonamide by reacting the monohalobiuret metal salt with ammonia; and an ammonia evaporator to separate the excess ammonia from hydrazodicarbonamide and to supply the separated ammonia to an ammonia concentrator.

REFERENCES:
Waki, Kunio; Haraguchi, Mitsuaki; Yamashita, Tadataka, The Thermal Decomposition of Hydrazodicarbamide, 1974, Nippon Kagaku Kaishi, 9, 1668-1672.

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