Apparatus for plasma synthesis of rhenium nano and micro...

Metallurgical apparatus – Means for treating ores or for extracting metals – By means applying heat to work – e.g. – furnace

Reexamination Certificate

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C219S121490

Reexamination Certificate

active

07910048

ABSTRACT:
The process for the synthesis of rhenium powders comprises the injection of ammonium perrhenate powder through a carrier gas in a plasma torch of a plasma reactor operated using a mixture including hydrogen as the plasma gas, yielding metallic rhenium under the following chemical reaction:in-line-formulae description="In-line Formulae" end="lead"?2NH4ReO4+4H2→2Re+N2↑+8H2O↑.in-line-formulae description="In-line Formulae" end="tail"?The reactor is provided with a quench zone for cooling the metallic rhenium so as to yield rhenium nano and micro powders.

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Tribalat S. Rhénium et technetium, Gauthier-Villars, Paris, 1957.
Davenport, William H. et al., “Rhenium Chemicals—Their Properties and Applications,” Cleveland Refractory Metals (Division, Chase Brass & Copper Co.), 1969.
Jungfleisch, M.L., et al., “Monographies sur les Métaux De Haute Pureté,” Masson et Cie, Éditeurs, 1972.

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