Apparatus for obtaining silicon from fluosilicic acid

Chemical apparatus and process disinfecting – deodorizing – preser – Chemical reactor – Including heat exchanger for reaction chamber or reactants...

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75844, 422241, 423350, B01J 1000, B01J 1926, C01B 3302, C22B 6100

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045979480

ABSTRACT:
Apparatus for producing low cost, high purity solar grade Si wherein a reduction reaction, preferably the reduction of SiF.sub.4, by an alkali metal (Na preferred) is carried out by jetting a spray of reactants into a reaction chamber at a rate and temperature which causes the reaction to take place far enough away from the entry region to avoid plugging of reactants at the entry region and wherein separation in the melt is carried out continuously from the reaction and the Si can be cast directly from the melt. The melt separation is provided by openings in the reaction chamber wall between about 2 and 3.5 millimeters in width. The Si is retained within the reaction chamber due to its surface tension.

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