Apparatus for direct melt synthesis of compounds containing vola

Chemistry: physical processes – Physical processes – Crystallization

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23273SP, 23290, 432262, B01D 900, B01J 300, F27B 1410

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active

039334350

ABSTRACT:
Apparatus for the melt synthesis of inorganic compounds from elemental reactants, at least one of which is highly volatile at the temperature of the reaction. An enclosure means defining a reaction chamber and a reservoir-closure means containing the volatile elemental reactant form the reaction vessel which is sealed by a combination mechanical-liquid seal which is of a character to permit diffusion by high-pressure gas through it. Heating means are provided to effect at least three heating regimes: (I) liquefaction of a liquid sealant, (II) formation and maintenance of a molten reaction mass, and (III) heating of the volatile elemental reactant to vaporize it.

REFERENCES:
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patent: 2631091 (1953-03-01), Kuentzel et al.
patent: 3118737 (1964-01-01), Blocher, Jr.
patent: 3552931 (1971-01-01), Doherty et al.
patent: 3627499 (1971-12-01), Le Duc et al.
patent: 3825242 (1974-07-01), Menashi et al.

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