Apparatus for depleted chemical milling solutions

Liquid purification or separation – Constituent mixture variation responsive

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Details

210178, 210196, 210202, 210266, B01D 3604

Patent

active

049605119

ABSTRACT:
A process is disclosed for removing heavy metals, dissolved aluminum, sulfides and organic compounds from a caustic etch solution, thereby regenerating the etching power of the solution or facilitating its disposal into the environment. The process consists of forming a first filtrate from which heavy metals present in the solution have been removed, and a second filtrate obtained by precipitating and oxidizing residual chemicals remaining in the first filtrate. The latter is done over a selected pH and temperature range. The second filtrate is then either reclaimed back to the etching tank, or subjected to ozonization prior to disposing of it into the environment.

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Dejak, "Aluminum Anodizer Regenerates Caustic Etch Solution", Plating and Surface Finishing, 30-32 (Apr. 1984).
Brown, "Recovery of Aluminum Finishing Wastes", Industrial Finishing, 50-60, (Oct., 1982).

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