Apparatus for controlling the directional solidification of a li

Chemical apparatus and process disinfecting – deodorizing – preser – Chemical reactor – Including specific material of construction

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156601, 156616R, 156607, 156622, 73 15R, 73 3, 73 17R, 73296, 73433, 73437, 116216, 116217, 432 45, 356372, B01J 1708

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041972732

ABSTRACT:
The growth of a solid obtained by cooling a liquid solution is observed and controlled by measuring the variation in volume of the solid-liquid system at the time of solidification. The method is applicable to the control of oriented crystallization from an initial crystal seed or epitaxial growth on a substrate having a suitable crystal orientation. The rate of crystallization can be controlled by means of a furnace provided with means for producing regulated thermal gradients, temperature-measuring means, a chamber filled with an inert liquid, an open-topped container filled with the liquid to be solidified and immersed in the inert liquid, the container being suspended from one arm of the beam of an electrobalance.

REFERENCES:
patent: 1800532 (1931-04-01), Howard
patent: 2135183 (1938-11-01), Junghans
patent: 2908004 (1959-10-01), Levinson
patent: 3459152 (1969-08-01), Garrison
patent: 3791887 (1974-02-01), Deitch
patent: 3822111 (1974-07-01), Suzuki
patent: 3859856 (1975-01-01), Keele
patent: 3879235 (1975-04-01), Gatos
patent: 3934983 (1976-01-01), Bardsley
patent: 4132186 (1979-01-01), Manske
Bardsley et al., Journal of Crystal Growth, 24/25, Mar. 1974, pp. 369-373.

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