Apparatus for continuous overbasing of petroleum sulfonate with

Chemical apparatus and process disinfecting – deodorizing – preser – Analyzer – structured indicator – or manipulative laboratory... – Automatic analytical monitor and control of industrial process

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422111, 422189, 422225, 422234, 436 55, 436131, B01J 1000, B01F 304

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046613188

ABSTRACT:
A method and apparatus for the continuous overbasing of petroleum sulfonate providing in a process in which CO.sub.2 is contacted with a reaction mixture of neutral petroleum sulfonate, lube oil stock, lime, methanol, and naphtha in a series of reaction vessels in which additional CO.sub.2 is contacted seriatim in each succeeding reaction vessel with the effluent from the preceding reaction vessel, a method and apparatus for the removal of at least a portion of the effluent from each reaction vessel with the reduction of water content in this portion and subsequent supplementing of methanol content in this portion to provide a reaction efficient amount of water and methanol in each succeeding reaction.

REFERENCES:
patent: 2663699 (1953-12-01), Bloem et al.
patent: 2880076 (1959-03-01), Kircher, Jr. et al.
patent: 2978441 (1961-04-01), Sherk
patent: 3878116 (1975-04-01), Rueckert
patent: 3896037 (1975-07-01), Dickey
patent: 4291132 (1981-09-01), Clifford

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