Apparatus and process for conducting combinational chemical synt

Chemical apparatus and process disinfecting – deodorizing – preser – Chemical reactor – Including means rotating reaction chamber during use

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4352867, 4352884, 436518, B01J 808

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active

059808390

ABSTRACT:
The objective of combinatorial chemical synthesis is the preparation of a very large number of different molecular entities by a randomized process of sequential chemical syntheses. The present invention provides a combinatorial vessel comprising a reaction region and a mixing region, adjacent to each other, which can be used to practice combinatorial chemical synthesis. The reaction region comprises a plurality of reaction cavities, in which a plurality of different chemical reactions may be performed simultaneously on resin beads. The resin beads are then transferred to the mixing region and mixed into a single group. Then, the resin beads are transferred into the reaction cavities. The process of performing reactions, transferring to the mixing region, mixing, and transferring to the reaction region can be repeated multiple times to obtain a large number of resin beads, each of which has been exposed to a series of reactions different from most of the other resin beads.

REFERENCES:
A. Furka et al., Int'l Abstract No. P-168, Xth Int'l Symp. Med. Chem., Budapest, Hungary, Aug. 1988.
A. Furka et al., Int'l J. Peptide Protein Res., vol. 37, pp. 487-493, 1991.
A. Furka et al., "Proteins and Nucleic Acids in Three Dimensions," 14th Int'l Congress of Biochemistry, Abstracts, vol. 5, FR: 013, Prague, Czechoslovakia, Jul. 15, 1988.
R.N. Zuckermann et al., Int'l J. Peptide Protein Res., vol. 40, pp. 497-506 (1992).
Z. Moukheiber, "A Hail of Silver Bullets," Forbes, pp. 76-81, Jan. 26, 1998.
C. Wrotnowski, "Important Trends and Developments in Biotechnology Instrumentation Systems," Genetic Engineering News, pp. 6 and 35, Dec. 1997.
S. Danheiser, "Laboratory Automation and Robotics to Play A Major Role in the Drug Discovery Process," Genetic Engineering News, pp. 1 & 10, Dec. 1997.

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