Apparatus and method for verification of monophasic samples

Wells – Processes – With indicating – testing – measuring or locating

Reexamination Certificate

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Details

C166S064000, C166S264000, C073S152280

Reexamination Certificate

active

06216782

ABSTRACT:

TECHNICAL FIELD OF THE INVENTION
This invention relates in general to testing and evaluation of subterranean formation fluids and, in particular to, a fluid sampling tool and method for monitoring the temperature of the sample to determine whether the sample has undergone phase change degradation during collection or retrieval from the wellbore.
BACKGROUND OF THE INVENTION
Without limiting the scope of the present invention, its background is described with reference to testing hydrocarbon formations, as an example.
It is well known in the subterranean well drilling and completion art to perform tests on formations intersected by a wellbore. Such tests are typically performed in order to determine geological or other physical properties of the formation and the chemical and physical properties of the fluids contained therein. For example, parameters such as permeability, porosity, fluid resistivity, temperature, pressure and bubble point may be determined. These and other characteristics of the formation and fluid contained therein may be determined by performing tests on the formation before the well is completed.
One type of testing procedure is to obtain a fluid sample from the formation to, among other things, determine the composition of the formation fluids. In this procedure, it is important to obtain a sample of the formation fluid that is representative of the fluids as they exist in the formation. For example, the sample is used to determine the economic value of fluids within the formation. In addition, the composition of the formation fluids is used to determine the type and capacity of the processing equipment required to process fluids extracted from the formation.
In the past, sampling of formation fluids was accomplished by collecting a large volume of fluid through the drill string which may be on the order of thousands of gallons of formation fluids. This type of large scale sampling is, however, timely and expensive. In an alternative sampling procedure, formation fluids may be sampled on a smaller scale by lowering a sampling tool into the wellbore on a wireline, slick line or tubing string. In this case, when the sampling tool reaches the desired depth, one or more ports are actuated from the closed position to the opened position to allow collection of the formation fluids. The ports may be actuated in variety of ways such as by electrical, hydraulic or mechanical methods. Once the ports are opened, formation fluids travel through the ports and a sample of the formation fluids is collected within a chamber of the sampling tool. After the sample has been collected, the sampling tool may be withdrawn from the wellbore so that the formation fluid sample may be analyzed.
It has been found, however, that with the use of conventional formation sampling tools, the fluid sample is obtained relatively quickly which can cause phase change degradation of the formation fluid due to flashing as the fluid flows into the sampling chamber. This phase change degradation may result in irreversible chemical and physical changes in the formation fluid. For example, in a typical sampling procedure, the formation fluids flow through one or more valves or passageways to enter the sampling chamber. The inherent pressure drop across the valves or passageways creates the possibility that lighter fractions present in the sample will flash, or come out of solution, during collection. Once flashing has occurred, the resulting sample may no longer be representative of the fluids present in the formation.
It has also been found that as conventional formation sampling tools are retrieved from the wellbore, the reduction in hydrostatic pressure acting on the sampling tool may result in a reduction of the fluid pressure within the sampling chamber. This drop in pressure may similarly cause phase change degradation of the sample as the sampling tool is removed from the wellbore. In the past, it has been difficult to know whether the sample has undergone phase change degradation either during collection or retrieval from the wellbore. As such, it has been difficult to determine whether the sample is representative of the fluids present in the formation.
Therefore, a need has arisen for an apparatus and method for obtaining a fluid sample from a formation without phase change degradation of the sample during collection or retrieval of the sampling tool from the wellbore. A need has also arisen for such an apparatus and method that is capable of verifying whether the sample has undergone phase change degradation.
SUMMARY OF THE INVENTION
The present invention disclosed herein provides a downhole sampling apparatus and a method for obtaining a fluid sample from a formation without the occurrence of phase change degradation of the sample during collection or retrieval of the sampling tool from the wellbore. The downhole sampling apparatus and method of the present invention is capable of verifying whether the sample has undergone phase change degradation by monitoring the temperature of the sample during collection and retrieval of the downhole sampling apparatus from the wellbore.
In one embodiment, the downhole sampling apparatus of the present invention comprises a housing having a sampling chamber and a sampling port defined therein. The sampling port is in communication with the sampling chamber and the formation traversed by the wellbore. A temperature monitoring device is at least partially disposed within the sampling chamber. The temperature monitoring device monitors the temperature of formation fluid collected in the sampling chamber to determine whether the formation fluid undergoes phase change degradation. The temperature monitoring device is operatively connected to a temperature recorder so that temperature fluctuations in the formation fluid may be recorded.
In another embodiment, the downhole sampling apparatus of the present invention comprises a housing having a fluid passageway that is in communication with the formation. A sampling device is disposed within the housing. The sampling device has a sampling chamber and a sampling port defined therein. The sampling port is in communication with the sampling chamber and the fluid passageway. A temperature recorder is also disposed within the housing. The temperature recorder includes a temperature monitoring device that is in communication with the fluid passageway for monitoring the temperature of formation fluid entering the sampling port.
In either embodiment, a check valve is disposed within the sampling port for allowing formation fluid flow through the sampling port into the sampling chamber while preventing reverse flow from the sampling chamber out through the sampling port. The sampling device may also include first and second operating fluid chambers. A control valve is disposed between the first and second operating fluid chambers for initially isolating the first operating fluid chamber from the second operating fluid chamber. When the control valve is actuated, the first operating fluid chamber is in communication with the second operating fluid chamber such that operating fluid flows from the first operating fluid chamber to the second operating fluid chamber. Once this has occurred, formation fluid may flow through the sampling port into the sampling chamber. A flow restrictor may be use to impede the rate of fluid flow from the first operating fluid chamber to the second operating fluid chamber. A floating piston may be disposed between the sampling chamber and the first operating fluid chamber.
The sampling device may also have an isolation valve that allows outside hydrostatic pressure into the sampling device after a predetermined volume of operating fluid has flowed from the first operating fluid chamber to the second operating fluid chamber. A check valve may be used to trap the hydrostatic pressure within the sampling device.
In one the method of the present invention, the sampling device is run into the wellbore to a depth at which the formation fluids are to be sampled. The sampling tool then collects f

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