Apparatus and method for preparing samples for radiocarbon...

Radiant energy – Methods including separation or nonradiant treatment of test...

Reexamination Certificate

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C436S059000, C422S083000

Reexamination Certificate

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10924672

ABSTRACT:
The invention provides a method and apparatus for preparing samples of carbon dioxide with a14C content for analysis in liquid scintillation counting equipment, the sample being of a known mass and being introduced into and substantially wholly absorbed into an absorption “cocktail”, absorption being completed at a stage before saturation of the absorbent occurs. The absorbent is contained in a vial which, when absorption has been completed, is transferred into the scintillation counting equipment without intermediate transfer of the contents.

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patent: 3944471 (1976-03-01), Waters
patent: 4019864 (1977-04-01), Saito et al.
patent: 5402834 (1995-04-01), Levin et al.
Thomson,J. Sample Preparation and Counting of Biological Samples, Packard Instrument Application Note AN9002-CSR, 1999.
Thomson,J. Sample Preparation and Counting of Biological Samples, Packard Instrument Application Note AN9002-CSR, 1999.
Leaney, et al., New Developments For The Direct CO, Absorption Method For Radiocarbon Analysis, Quarternary Geochronology/Quarternary Science Review, 1994, pp. 171-178, vol. 13, Elsevier Science Ltd., Great Britain.
Qureshi et al., The CO2absorption method as an alternative to benzene synthesis method for14C dating, Applied Geochemistry, 1989, pp. 625-633, vol. 4, Pergamons Press, Great Britain.
Aravena et al., New Possibilities for14C Measurements By Liquid Counting, Radiocarbon, 1989, pp. 387-392, vol. 31, No. 3, Geological Survey of Canada, Canada.

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