Apparatus and method for polymer characterization

Chemistry: analytical and immunological testing – Including chromatography

Reexamination Certificate

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C422S070000, C073S061520, C073S061560, C210S198200, C210S656000

Reexamination Certificate

active

07985593

ABSTRACT:
Apparatus for GPC/TREF and TREF/GPC characterization of a polymer sample. The apparatus provides for the automated and integrated use of multiple TREF columns and a GPC system employing a multiple flow through detectors. In addition, a method for TREF/GPC characterization of a polymer sample by GPC analysis of TREF fractions at increasing TREF elution temperatures from multiple TREF columns operated in a coordinated and synchronized temperature cycle for increased sample throughput. Also, a method for GPC/TREF characterization of a polymer sample by GPC fractionation followed by TREF fractionation of the GPC fractionations.

REFERENCES:
patent: 2006/0266708 (2006-11-01), Yu et al.
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Zacur, et al, Polymer Engineering and Science, vol. 39, No. 5, pp. 921-929 (1999).
Wild, et al, Journal of Polymer Science, vol. 20, pp. 441-455 (1982).
Yau, et al., 2000 Tappi Polymers, Laminations, & Coatings Conference, pp. 699-707 (2000).
Yau, et al., Polymer 42, pp. 8947-8958 (2001).
Wild, et al., Polymer Preparation, vol. 18, p. 182 (1977).

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