Apparatus and method for parallel coupling reactions

Chemical apparatus and process disinfecting – deodorizing – preser – Chemical reactor – Organic polymerization

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422110, 422116, 530333, 530334, 525 541, 525 5411, C08F 200, G05B 1700, C12N 1500, A61K 3800

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060569263

ABSTRACT:
A device and method for efficiently synthesizing diverse molecular products on substrates. A parent vessel 200 contains a suspension of substrates. The suspension is pressurized with argon and transferred to a plurality of reaction vessels 201-209 in one or more reaction vessel banks where monomer addition reactions take place. Optionally, the substrates may be tagged with a tag monomer. A vortexing motor 300 vortexes the contents of reaction vessels 201-209 during monomer addition reactions to enhance synthesis. After the desired monomer and/or tag monomer addition reaction, the suspension is pressurized with argon and transferred back to parent vessel 200 for mixing. Thereafter, the suspension may be pressurized with argon and reallocated among reaction vessels 201-209 for further synthesis.

REFERENCES:
patent: 4182654 (1980-01-01), Royer
patent: 4315074 (1982-02-01), Royer
patent: 4517338 (1985-05-01), Urdea et al.
patent: 4587044 (1986-05-01), Miller et al.
patent: 4631211 (1986-12-01), Houghten
patent: 4671941 (1987-06-01), Niina et al.
patent: 4671947 (1987-06-01), Niina et al.
patent: 4701304 (1987-10-01), Horn et al.
patent: 4704256 (1987-11-01), Hood et al.
patent: 4713326 (1987-12-01), Dattagupta et al.
patent: 4746490 (1988-05-01), Saneii
patent: 4755558 (1988-07-01), Kalbag
patent: 4794150 (1988-12-01), Steel
patent: 4812654 (1989-03-01), Royer
patent: 4818681 (1989-04-01), Dattagupta
patent: 4833092 (1989-05-01), Geysen
patent: 4855225 (1989-08-01), Fung et al.
patent: 4965188 (1990-10-01), Mullis et al.
patent: 5143854 (1992-09-01), Pirrung et al.
patent: 5182366 (1993-01-01), Hueber et al.
patent: 5252296 (1993-10-01), Zuckermann et al.
patent: 5264563 (1993-11-01), Huse
patent: 5324483 (1994-06-01), Cody et al.
Advances in Analytical Chemisrty and Instrumentation, Charles N. Reilley, Ed., John Wiley & Sons, Inc., 1964, pp. 56-59.
Arnold et al., Mar. 15, 1991, Optics Letters 16(6):420-422 Room-temperature microparticle-based persistent spectral hole burning memory.
Baldwin et al., 1990, Tetrahedron 46(19):6879-6884 New photolabile phosphate protecting groups.
Barr et al., 1986, BioTechniques 4(5):428-432 7-Deaze-2'-deoxyguanosine-5'-triphosphate: Enhanced resolution in M13 dideoxy sequencing.
Bashkin et al., 1991, J. Org. Chem. 56:3168-3176 Synthesis and characterization of oligonucleotide peptides.
Borchardt et al., 1994, J. Am. Chem. Soc. 116:373-374 Synthetic receptor binding elucidated with an encoded combinatorial library.
Brenner et al., 1992, Proc. Natl. Acad. Sci. USA 89:5381-5383 Encoded combinatorial chemistry.
Crick et al., 1957, Proc. Natl. Acad. Sci. USA 43:416-421 Codes without commas.
Cwirla et al., 1990, Proc. Natl. Acad. Sci. USA 87:6378-6382 Peptides on phage: A vast library of peptides for indentifying ligands.
Eritja et al., 1991, Tetrahedron 47(24):4113-4120 Synthesis of defined peptide-oligonucleotide hybrids containing a nuclear transport signal sequence.
Fodor et al., 1991, Science 251:767-773 Light-directed, spatially addressable parallel chemical synthesis.
Frank and Doring, 1988, Tetrahedron 44(19):6031-6040 Simultaneous multiple peptide synthesis under continuous flow conditions on cellulose paper discs as segmental solid supports.
Frank et al., 1983, Nuc. Acids. Res. 11(13):4365-4377 A new general approach for the simultaneous chemical synthesis of large numbers of oligonucleotides: Segmental solid supports.
Frank et al., 1990, Peptides (Giralt & Andreu, eds., Escom Science Pub.), pp. 151-152 Facile and rapid `spot-synthesis` of large numbers of peptides on membrane sheets.
Furka et al., Jul. 10-15, 1988, 14th Int'l Congress of Biochemistry, Prague, Czechoslovakia, Abstract No. FR:013 Proteins and nucleic acids in three dimensions: Cornucopia of peptides by synthesis.
Furka et al., Aug. 15-19, 1988, Symp. on Medicinal Chem., Budapest, Hungary, Abstract No. P-168, p. 288 More peptides by less labour.
Furka et al., 1991, Int. J. Peptide Protein Res., 37:487-493 General method for rapid synthesis of multicomponent peptide mixtures.
Geysen et al., 1987, J. Immunol. Meth., 102:259-274 Strategies for epitope analysis using peptide synthesis.
Geysen et al., 1984, Proc. Natl. Acad. Sci. USA, 81:3998-4002 Use of peptide synthesis to probe viral antigens for epitopes to a resolution of a single amino acid.
Haralambidis et al., 1990, Nuc. Acids Res. 18(3):493-505 The synthesis of polyamide-oligonucleotide conjugate molecules.
Hayakawa et al., 1990, J. Am. Chem. Soc. 112:1691-1696 The allylic protection method in solid-phase oligonecleotide synthesis: An efficient preparation of solid-anchored DNA Oligomers.
Hodgson, 1992, Bio/Technology 10:973-974 Receptor screening and the search for new pharmaceuticals.
Houghten et al., 1991, Nature 354:84-86 Generation and use of synthetic peptide combinatorial libraries for basic research and drug discovery.
Houghten, 1985, Proc. Natl. Acad. Sci. USA 82:5131-5135 General method for the rapid solid-phase synthesis of large numbers of peptides: Specificity of antigen-antibody interaction at the level of individual amino acids.
Juby et al., 1991, Tetrahedron Letters 32(7):879-882 Facile preparation of 3' oligonucleotide-peptide conjugates.
Kaiser et al., 1989, Science 243:187-192 Peptide and protein synthesis by segment synthesis-condensation.
Kerr et al., 1993, J. Am. Chem Soc., 115:2529-2531 Encoded combinatorial peptide libraries containing non-natural amino acids.
Lam et al., 1991, 12th Amer. Pep. Symp., Abstract LW3 Rapid selection and structure determination of acceptor binding ligands from a large synthetic peptide library.
Lam et al., 1991, Nature 354:82-84 A new type of synthetic peptide library for indentifying ligand-binding activity.
Needels et al., 1993, Proc. Natl. Acad. Sci. USA, 90:10700-10704 Generation and screening of an oligonucleotide-encoded synthetic peptide library.
Nikolaiev et al., 1993, Peptide Research, 6(3):161-170 Peptide-encoding for structure determination of nonsequenceable polymers within libraries synthesized and tested on solid phase supports.
Ohlmeyer et al., 1993, Proc. Natl. Acad. Sci. USA, 90:10922-10926 Complex synthetic chemical libraries indexed with molecular tags.
Tjoeng et al., 1990, Int. J. Pept. Protein Res. 35:141-146 Multiple peptide synthesis using a single support (MPS3).
Van der Zee et al., 1989, Eur. J. Immunol. 19:43-48 Efficient mapping and characterization of a T cell epitope by the simultaneous synthesis of multiple peptides.

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