Drying and gas or vapor contact with solids – Apparatus – With automatic control
Reexamination Certificate
2001-08-28
2004-07-27
Weier, Anthony J. (Department: 1761)
Drying and gas or vapor contact with solids
Apparatus
With automatic control
C034S527000, C034S573000, C034S549000, C034S535000, C034S164000, C034S165000, C034S168000, C034S171000, C034S090000, C034S092000
Reexamination Certificate
active
06766595
ABSTRACT:
TECHNICAL FIELD
This invention relates to a material treating apparatus and method, and more particularly to an apparatus and method for heat treating a solvent extracted oleaginous material for enhanced recovery of solvent and steam used in the heat treating process. The apparatus and method are also applicable to the thermal treatment of other materials and to materials containing liquids adhering thereon.
BACKGROUND OF INVENTION
In the processing of oleaginous seeds to extract oil by solvent extraction, the seeds are crushed, milled or otherwise fragmented (i.e., made into cakes, flakes etc.) and are treated with a solvent to extract the oil, leaving a solvent extracted material (i.e., a particulate material, e.g., a meal) in which vaporizable solvent remains. By heating the meal using steam both indirectly as by a heated surface and/or directly by intimate steam contact with the meal, the solvent is removed therefrom by vaporization while the “wet” meal is dried and otherwise processed to deactivate certain types of enzymes and to denature proteins to thereby produce an edible substance.
The prior art generally discloses processes and apparatus wherein the material from which the solvent is to be removed progresses downwardly as a bed through a column which is provided with spaced horizontal plates therein dividing the interior of the column into a vertical series of compartments. In these compartments, the material is heated and agitated, with the finished material discharged from the bottom of the column and the solvent being removed as an overhead vapor from the column for subsequent condensing, with or without pre-conditioning or treatment.
Present desolventizing practice includes counter-current processing using a direct contacting flow of steam. Steam is distributed within the column such that it condenses on the particulate material while vaporizing some quantity of solvent adhered thereupon, further providing sensible heat to raise the temperature of the particulate material.
Generally, the moisture content of the particulate material exiting the desolventizer is from about 15 to 25 weight percent and is a function of prior solvent content, other moisture content, the ratio of direct steam to indirect steam used in the process, and the exit temperature. Drying is generally required to produce commercially saleable meal, with moisture reduction on the order of 25 to 33 percent being necessary so as to produce a commercial product having a moisture content of about 10-12 weight percent.
A shortcoming of known desolventizing practice is a small but significant quantity of the moisture content needing to be removed from the meal exiting the desolventizer is solvent. Customarily, a portion of the residual solvent remaining with the meal after desolventizing is driven off (i.e., vaporized) in subsequent drying steps, along with the condensed steam adhered or carried by the meal exiting the desolventizer.
Heretofore, no known desolventizing process or single apparatus has satisfactorily minimized atmospheric solvent vapor discharge, reduced the quantities of make-up to the recycle solvent stream and reduced the capital and operating costs of desolventizing operations as contemplated by the apparatus and process of this invention.
SUMMARY OF THE INVENTION
It is a first objective of the invention to provide an improved apparatus and method for desolventizing a particulate material.
Another objective of the invention is to provide an improved apparatus and method for desolventizing a particulate material whereby solvents are substantially vaporized in an indirect heating zone and further vaporized in a direct heating zone.
Another objective of the invention is to provide an improved apparatus and method for enhanced solvent vapor recovery from a particulate material having a solvent carried thereby, whereby particulate material in a direct heating zone enters an integral air tight flash chamber positioned below a live steam sparge tray prior to discharge of the “wet” solvent extracted material from the desolventizer.
Another objective of the invention is to provide an improved apparatus and method for more efficiently heat treating a solvent extracted material to remove the solvent adhered thereto whereby residual solvent vapor obtained in a flash chamber integral to a desolventizer is thermocompressed for entry into a direct heating zone.
According to a preferred embodiment of the present invention and in furtherance of aforementioned objectives, apparatus and method is provided having an upper indirect heating zone and a lower direct heating zone. Each of the zones has a plurality of spaced apart horizontal trays for receiving particulate material. The trays of the indirect heating zone permit flow of solvent vapor theraround while the trays of the direct heating zone allow a counter-current flow of solvent vapor and steam therethrough. The trays define a vertical series of compartments through which particulate material passes. Separate means for providing steam to the particulate material indirectly in said indirect heating zone and directly in said direct heating zone are provided. An integral air tight flash chamber below the means for providing steam heat to the particulate material directly in said direct heating zone enhances solvent recovery via vaporization of residual solvent from the condensed steam adhered to the particulate material traveling through the direct heating zone prior to discharge of the particulate material for subsequent processing. Means for delivering the vaporized residual solvent under pressure to a predetermined compartment in the direct heating zone provide heat for desolventizing the particulate material.
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Crown Iron Works Company
Nawrocki, Rooney & Sivertson P.A.
Weier Anthony J.
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