Anhydrous magnesium chloride using ethylene glycol and ammonia

Details Anhydrous magnesium chloride using ethylene glycol and ammonia Anhydrous magnesium chloride using ethylene glycol and ammonia

1975-10-29

1976-06-29

Stern, Edward

Chemistry of inorganic compounds

Halogen or compound thereof

Binary compound containing metal

423351, C01F 534

Patent

active

039668886

ABSTRACT:
Anhydrous magnesium chloride may be prepared from magnesium chloride hydrates by the following sequence of processing steps:
1. Dissolving the magnesium chloride hydrate in ethylene glycol to form a magnesium chloride hydrate solution.
2. Heating the thus-formed solution to remove all the water therefrom thereby forming a ethylene glycol anhydrous magnesium chloride solution.
3. Treating the water-free magnesium chloride-ethylene glycol solution with ammonia to form a magnesium chloride ammonia complex which precipitates from the ethylene glycol.
4. Removing the precipitate from the ethylene glycol and washing it with a low boiling solvent for ethylene glycol to remove any ethylene glycol entrained in the precipitate.
5. Heating the magnesium chloride ammonia complex to drive off the ammonia which leaves as a finished product completely anhydrous magnesium chloride.

REFERENCES:
patent: 3092450 (1963-06-01), Christensen
patent: 3352634 (1967-11-01), Buchmann
patent: 3594120 (1971-07-01), Bott et al.

Affiliated with

Also associated with

Rating

Anhydrous magnesium chloride using ethylene glycol and ammonia does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Anhydrous magnesium chloride using ethylene glycol and ammonia, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Anhydrous magnesium chloride using ethylene glycol and ammonia will most certainly appreciate the feedback.

Rate now

Comments { 0 }

Profile ID: LFUS-PAI-O-1278365