Analytical apparatus for determining volatiles, solids, and solv

Chemical apparatus and process disinfecting – deodorizing – preser – Analyzer – structured indicator – or manipulative laboratory... – Means for analyzing liquid or solid sample

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73 76, 422 74, 422 78, 436 43, 436178, G01N 504, G01N 2200, G01N 2204, G01N 2514

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active

045541329

ABSTRACT:
An apparatus and method for quantitatively measuring volatiles, solids and solvent extractables is described which provides rapid and accurate determinations using microwave heating, electronic balance weighing and solvent extracting of solubles. The method involves subjecting a weighed sample to microwave drying for a preselected time, reweighing to obtain the dry weight and determine volatile loss, solvent extracting the dried sample to determine fats, oils and other extractables followed by final measurement of residual solids. The apparatus is preferably automated to sequentially actuate the required weighing, microwave heating, solvent extraction, redrying, reweighing and calculation of the percentages of volatiles, solvent solubles and solids.
The apparatus and method are particularly suited for analytical uses in the food and dairy industries.

REFERENCES:
patent: 1255329 (1918-02-01), Mojonnier
patent: 3136609 (1964-06-01), Ciagne
patent: 3673852 (1972-07-01), Davis
patent: 3752651 (1973-08-01), Bush
patent: 3813918 (1974-06-01), Moe
patent: 3890825 (1975-06-01), Davis
patent: 3909598 (1975-09-01), Collins et al.
patent: 4072275 (1978-02-01), Bartels et al.
patent: 4106329 (1978-08-01), Tabahashi et al.
patent: 4165633 (1979-08-01), Raisanen
patent: 4168623 (1979-09-01), Thomas
patent: 4203727 (1980-05-01), Simpson
patent: 4246184 (1981-01-01), Pressick et al.
Chemistry and Testing of Dairy Products, Chapters 4 and 5, pp. 71-137, 1977.

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