Anaerobic curing composition and process for preparing same

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Polymers from only ethylenic monomers or processes of...

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526220, 526279, 526281, 526301, 526304, 526312, 526320, 5263231, 5263232, C08F 2214

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active

042152097

ABSTRACT:
Improved storage-stable anaerobic curing adhesive compositions useful as anaerobic adhesives and sealants are prepared by first mixing a polymerizable acrylate ester monomer, an inhibitor for free radical polymerization, a chelator, and at least an effective amount of an accelerator system consisting of an N-substituted sulfonamide and an aromatic tertiary amine. The resultant homogeneous mixture is thereafter maintained at a temperature of at least about 20.degree. C. for a period of time sufficient to provide the composition with anaerobic curing properties and a specified minimum amount of active oxygen. In one embodiment, the mixture is stirred at a temperature of 45.degree.-80.degree. C. for 10-30 hours. In another embodiment, the mixture is maintained at an elevated temperature without stirring.

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patent: 3795641 (1974-03-01), Lees et al.
patent: 3985943 (1976-10-01), Gruber et al.
patent: 4038475 (1977-07-01), Frauenglass et al.

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