Aluminum reference electrode

Chemistry: electrical and wave energy – Processes and products

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204 67, 204400, 204435, G01N 2746

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active

047642572

ABSTRACT:
A stable reference electrode for use in monitoring and controlling the process of electrolytic reduction of a metal. In the case of Hall cell reduction of aluminum, the reference electrode comprises a pool of molten aluminum and a solution of molten cryolite, Na.sub.3 AlF.sub.6, wherein the electrical connection to the molten aluminum does not contact the highly corrosive molten salt solution. This is accomplished by altering the density of either the aluminum (decreasing the density) or the electrolyte (increasing the density) so that the aluminum floats on top of the molten salt solution.

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patent: 4601810 (1986-07-01), Tiwari et al.
patent: 4645571 (1987-02-01), Dubreuil et al.
Aluminum Electrolysis-Fundamentals of the Hall-Heroult Process, (2nd Ed.), K. Grjotheim et al, pp. 128-139, 184-215 (1982).
"Zur Elektrometallurgie Des Aluminiums", Paul Dro bach, Ztschr. Electrochem, Bd. 42, Nr. 2 (1936), pp. 65-70.
"Aluminum/Cryolite Reference Electrodes for Use in Cryolite-Based Melts", John W. Burgman et al, J. Electrochem. Soc.: Electrochemical Science and Technology, pp. 496-500, Mar. 1986.
"Handbook of Chemistry & Physics", 55th ed., pp. B-63 & B-138.

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