Coating apparatus – Control means responsive to a randomly occurring sensed... – Temperature responsive
Patent
1995-10-12
1996-07-30
Bueker, Richard
Coating apparatus
Control means responsive to a randomly occurring sensed...
Temperature responsive
118668, 118708, 118712, 118715, 118719, 118726, C23C 1600
Patent
active
055407773
ABSTRACT:
A process and apparatus for Al.sub.2 O.sub.3 CVD on silicon wafers using aluminum tri-isopropoxide in a high-volume production environment is presented. The conditions required to use ATI in a production environment and provide maximum utilization of ATI are first of all delivery of ATI via direct evaporation. The ATI source bottle is pumped out (bypassing substrates) until propene and isopropanol signals are reduced to 1% of process pressure before start of aluminum oxide deposition. Either IR spectroscopy or mass spectrometry can be used to provide a control signal to the microprocessor controller. Heating the supplied tetramer to 120.degree. C. for two hours assures complete conversion to trimer. The ATI is stored at 90.degree. C. to minimize decomposition during idle periods and allow recovery of trimer upon return to 120.degree. C. for two hours. During periods of demand, the ATI is held at 120.degree. C. to minimize decomposition.
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Barbee Steven G.
Chapple-Sokol Jonathan D.
Conti Richard A.
Hsiao Richard
O'Neill James A.
Bueker Richard
International Business Machines - Corporation
Mortinger Alison
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