Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1993-07-06
1994-07-26
Dees, Jose G.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
C07F 102
Patent
active
053325338
ABSTRACT:
A high temperature process for producing alkyllithium compounds in high yields of at least 90% and high purity comprising reacting, in a liquid hydrocarbon solvent, an alkyl halide containing 3 to 16 carbon atoms and mixtures thereof with lithium metal particles of less than 300 microns in size at a temperature between 35.degree. and 125.degree. C. and recovering the alkyllithium compound.
REFERENCES:
patent: 3122592 (1964-02-01), Eberly
patent: 3452112 (1969-07-01), Kamienski
Conrad W. Kamienski, The Journal of Organic Chemistry, vol. 34, (1969) No. 4, pp. 1116-1121.
Henry Gilman et al., Journal of American Chemical Society, vol. 63, pp. 2479-2482 (1941).
Henry Gilman et al., Journal of American Chemical Society, vol. 62 pp. 2327-2335 (1940).
Cong-yuan Guo, Journal of American Chemical Society, 1985, 107, pp. 6028-6030.
Robert N. Mealsi, The Journal of Organic Chemistry, vol. 9, pp. 211-218 (1944).
Dover B. Troy
Engel John F.
Hall Randy W.
Kamienski Conrad W.
Morrison Robert C.
Andersen Robert L.
Dees Jos,e G.
Fellows Charles C.
FMC Corporation
Nazario-Gonzalez Porfirio
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