Alkyl-phenylcarbamate derivative of polysaccharide

Organic compounds -- part of the class 532-570 series – Organic compounds – Carbohydrates or derivatives

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106162, 1061631, 106210, 106205, 106208, 210656, 536 20, 536 30, 536 45, 536 51, C08B 1506, C08B 3300, C08B 3702, C08B 3708

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048618721

ABSTRACT:
An alkyl-phenylcarbamate derivative of a polysaccharide has in 80 to 100 percent of hydrogen atoms of the amino and hydroxyl groups an alkylphenyl-carbamoyl group having the formula (I): ##STR1## in which (1) at least one of R1 to R5 is a straight alkyl having 4 to 8 or a branched alkyl having 3 to 8 carbon atoms or at least two of R1 to R5 each are a straight alkyl having 1 to 3 when the polysaccharide is cellulose; (2) at least one of R1 to R5 is a straight alkyl having 1 to 8 carbon atoms or a branched alkyl having 3 to 8 carbon atoms when the polysaccharide is any one other than cellulose; and the other(s) of R1 to R5 is hydrogen. It is useful to optical separation of a racemic mixture.

REFERENCES:
McCormick et al., "Homogeneous Solution Reactions of Cellulose, Chitin, and Other Polysaccharides", 1980 American Chemical Society, pp. 372-380.
Yoshio Okamoto et al, "Controlled Chiral Recognition of Cellulose Triphenylcarbamate Derivatives Supported on Silica Gel", 1986 Journal of Chromatography, pp. 173-186.

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