Alkyl 2-fluoro-1-methoxyethylcarbamates

Details Alkyl 2-fluoro-1-methoxyethylcarbamates Alkyl 2-fluoro-1-methoxyethylcarbamates

1988-02-11

1989-07-04

Lone, Warren B.

Organic compounds -- part of the class 532-570 series

Organic compounds

Carboxylic acid esters

560161, 562555, C07C12504

Patent

active

048452670

ABSTRACT:
Alkyl esters of 2-fluoro-1-methoxyethylcarbamic acid, which are useful intermediates in the preparation of compounds, such as 4-amino-5- fluoropentanoic acid, are prepared by the electrochemical anodic oxidation of esters of 2-fluoroethylcarbamic acid in the presence of methanol and an electrolyte.

REFERENCES:
patent: 4326071 (1982-04-01), Bey et al.
patent: 4528028 (1985-07-01), Flint et al.
T. Shono et al., J. Am. Chem. Soc. 97, 4264 (1975).
T. Shono et al., J. Org. Chem. 52, 536 (1987).
T. Fuchigami et al., J. Org. Chem. 52, 5489 (1987).
T. Fuchigami et al., Tetrahedron Letters 27, 3869 (1986).
Eberson and Utley in Organic Electrochemistry 2nd Ed., pp. 779-783, 1983, edited by M. Baiser and H. Lund, 1983.
R. B. Silverman et al., J. Org. Chem. 45, 815 (1980).

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