Alkene intermediates and synthesis thereof

Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing

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556482, 558210, C07C 4302, C07F 704, C07F 902

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active

059361328

ABSTRACT:
A chemiluminescent 1,2-dioxetane derivative having a formula (I): ##STR1## wherein R.sup.1 and R.sup.4 each represent, individually, hydrogen, an alkyl group, an alkoxyl group, a hydroxyl group, or --OS;(R.sup.9 R.sup.10 R.sup.11) in which R.sup.9, R.sup.10 and R.sup.11 each represent an alkyl group; R.sup.2, R.sup.3, R.sup.5 and R.sup.6 each represent, individually, hydrogen or an alkyl group, provided that R.sup.2, R.sup.3, R.sup.5 and R.sup.6 each cannot be hydrogen at the same time, and that R.sup.2 and R.sup.3, and R.sup.5 and R.sup.6, each taken together, can form a cycloalkyl group; R.sup.7 represents an alkyl group; R.sup.8 represents hydrogen, an alkoxyl group, a phosphate salt group, or --OSi(R.sup.9 R.sup.10 R.sup.11); intermediates for synthesizing the above 1,2-dioxetane derivative; and methods of producing the intermediates are provided.

REFERENCES:
Journal of Heterocyclic Chemistry, vol. 14, No. 2, Apr. 1997, PROVO US pp. 181-184.
Journal of the Chemical Society, Chemical Communications, vol. 21, Nov. 7, 1994, Letchworth GB pp. 2449-2450.
Matsumoto, M. et al "Thetmal stability and chemiluminescence of 3-alkoxy-3-aryl-4,4-diisopropyl-1,2-dioxetanes" CA 122:313997, 1995.

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