Alkali metal hydride formation

Chemistry of inorganic compounds – Hydrogen or compound thereof – Binary compound

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423648, 2521883R, 23290, C01B 604, C01B 102

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active

040072576

ABSTRACT:
The present invention relates to a method of producing alkali metal hydrides by absorbing hydrogen gas under pressure into a mixture of lower alkyl mono amines and alkali metal alkyl amides selected from sodium and potassium amides formed from said amines. The present invention also includes purification of a mixture of the amines and amides which contain impurities, such as is used as a catalytic exchange liquid in the enrichment of deuterium, involving the formation of the alkali metal hydride.

REFERENCES:
patent: 2378368 (1945-06-01), Alexander
patent: 3595617 (1971-07-01), Vit et al.
patent: 3617218 (1971-11-01), Van Tamelin et al.
Bar-Eli et al., "Journal of the Chemical Soc., " Aug. 1962, pp. 3083-3088.
Jickling, "AECL Res. Eng. (Canada)", Feb. 1971, pp. 2-4.

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