9- (substituted amino) -alpha-6-deoxy-5-oxy tetracycline derivat

Drug – bio-affecting and body treating compositions – Designated organic active ingredient containing – 3,10-dihydroxy-2-naphthacene carboxamide or derivative doai

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514445, 552204, 552205, 549 65, A01N 3718, C07C23726

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active

058344500

DESCRIPTION:

BRIEF SUMMARY
This application is a 371 of PCT/IB95/00026 filed Jan. 12, 1995.
This invention relates to novel doxycline analogs that exhibit antibiotic activity against a wide range of gram-positive and gram-negative organisms, including organisms that are resistant to tetracycline antiobiotics.
Doxycycline (.alpha.-6-deoxy-5-oxytetracycline) and other 6-deoxytetracyclines are referred to in articles by Stephens et al., J. Amer. Chem. Soc., 85, 2643-2652 (Sep. 5, 1963) and Petisi et al., J. Med. Pharm. Chem., 5 538 (1962). They are also referred to in U.S. Pat. No. 3,200,149, which issued on Aug. 10, 1965.
European Patent Application 536515A1, which was published on Apr. 14, 1993, refers to 7-substituted-9-(substituted amino)6-demethyl-6-deoxytetracycline compounds that exhibit activity against a wide spectrum of organisms including organisms that are resistant to tetracyclines. This application and the foregoing references are incorporated herein by reference in their entireties.


SUMMARY OF THE INVENTION

This invention relates to compounds of the formula ##STR2## wherein R.sup.1 is hydrogen or --CH.sub.2 NR.sup.5 R.sup.6 ;
R.sup.2 is hydrogen or R.sup.4 (CH.sub.2).sub.n CO--;
n is an integer from 0 to 4;
R.sup.3 is R.sup.8 (CH.sub.2).sub.m CO-- or R.sup.8 (CH.sub.2).sub.m SO.sub.2 --;
m is an integer from 0 to 4;
and when n is 0, then either:
(a) R.sup.4 is selected from hydrogen; amino; monosubstituted amino selected from straight or branched (C.sub.1 -C.sub.6)alkylamino, cyclopropylamino, cyclobutylamino, benzylamino and phenylamino; disubstituted amino selected from dimethylamino, diethylamino, ethyl(1-methylethyl)amino, monomethylbenzylamino, piperidinyl, morpholinyl, 1-imidazolyl, 1-pyrrolyl, 1-(1,2,3-triazolyl) and 4-(1,2,4-triazolyl); straight or branched (C.sub.1 -C.sub.4)alkyl selected from methyl, ethyl, n-propyl, 1-methylethyl, n-butyl, 1-methylpropyl, 2-methylpropyl and 1,1-dimethylethyl; (C.sub.3 -C.sub.6)cycloalkyl selected from cyclopropyl, cyclobutyl, cyclopentyl and cyclohexyl; substituted (C.sub.3 -C.sub.6)cycloalkyl (substitution selected from (C.sub.1 -C.sub.3)alkyl, cyano, amino and (C.sub.1 -C.sub.3)acyl); (C.sub.6 -C.sub.10)aryl selected from phenyl, .alpha.-naphthyl and .beta.-naphthyl; substituted (C.sub.6 -C.sub.10)aryl (substitution selected from halo, (C.sub.1 -C.sub.4)alkoxy, trihalo(C.sub.1 -C.sub.3)alkyl, nitro, amino, cyano, (C.sub.1 -C.sub.4)alkoxycarbonyl, (C.sub.1 -C.sub.3)alkylamino and carboxy); (C.sub.7 -C.sub.9)aralkyl selected from benzyl, 1-phenylethyl, 2-phenylethyl and phenylpropyl; .alpha.-amino-(C.sub.1 -C.sub.4)alkyl selected from aminomethyl, .alpha.-aminoethyl, .alpha.-aminopropyl and .alpha.-aminobutyl; carboxy(C.sub.2 -C.sub.4)-alkylamino selected from aminoacetic acid, .alpha.-aminobutyric acid and .alpha.-aminopropionic acid and their optical isomers; (C.sub.7 -C.sub.9)aralkylamino (e.g., phenylglycyl); (C.sub.1 -C.sub.4)alkoxycarbonylamino substituted (C.sub.1 -C.sub.4)alkyl, substitution selected from phenyl and p-hydroxyphenyl; .alpha.-hydroxy(C.sub.1 -C.sub.3)alkyl selected from hydroxymethyl, .alpha.-hydroxyethyl, .alpha.-hydroxy-1-methylethyl and .alpha.-hydroxypropyl; .alpha.-mercaptopropyl; and halo-(C.sub.1 -C.sub.3)alkyl; or
(b) R.sup.4 is selected from Q.sup.1, Q.sup.2 and Q.sup.3, wherein Q.sup.1 is a five membered aromatic or saturated ring containing one N, O, S or Se heteroatom optionally having a benzo or pyrido ring fused thereto (e.g., ##STR3## wherein Z is N, O, S or Se);
Q.sup.2 is a five membered aromatic ring containing two heteroatoms independently selected from N, O, S and Se and optionally having a benzo or pyrido ring fused hereto (e.g., ##STR4## wherein Z and Z.sup.1 are independently selected from N, O, S and Se); and
Q.sup.3 is a five membered saturated ring containing one or two heteroatoms independently selected from N, O, S and Se and an adjacent appended O heteroatom (for example, ##STR5## wherein A is selected from hydrogen; straight or branched (C.sub.1 -C.sub.4)alkyl; C.sub.6 -aryl; substituted C.sub.6 -aryl (substitution select

REFERENCES:
patent: 5371076 (1994-12-01), Lee et al.

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