6-Ethylamino-2-picoline from 6-acetamido-2-picoline

Details 6-Ethylamino-2-picoline from 6-acetamido-2-picoline 6-Ethylamino-2-picoline from 6-acetamido-2-picoline

1976-03-15

1977-05-03

Randolph, John D.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260295AM, C07D21324

Patent

active

040214370

ABSTRACT:
Improvements in the reduction of 6-acetamido-2-picoline to produce 6-ethylamino-2-picoline, the improvements being in the use of diborane as the reducing agent and in the use of a low boiling petroleum solvent to separate the soluble 6-ethylamino-2-picoline from the insoluble starting material 6-acetamido-2-picoline. The 6-ethylamino-2-picoline final product is useful as an intermediate in a known method of preparing nalidixic acid, an antibacterial agent.

REFERENCES:
patent: 2894822 (1959-07-01), MacWood
Papanastassiou et al., J. Org. Chem. vol. 29, pp. 2870 to 2872 (1964).

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