5-carboxyl-1,3-diamino-2,4,6-trinitrobenzene and method of prepa

Details 5-carboxyl-1,3-diamino-2,4,6-trinitrobenzene and method of prepa 5-carboxyl-1,3-diamino-2,4,6-trinitrobenzene and method of prepa

1984-04-02

1991-10-01

Stoll, Robert L.

Organic compounds -- part of the class 532-570 series

Organic compounds

Nitriles

562437, 568933, C07C21149

Patent

active

H00009733

ABSTRACT:
5-carboxy-1,3-diamino-2,4,6-trinitrobenzene (DATBA), ##STR1## which is prepared by reacting 5-fluoro-1,3-diamino-2,4,6-trinitrobenzene with cyanotrimethylsilane to form 5-cyano-1,3-diamino-2,4,6-trinitrobenzene which is then hydrolyzed with a strong acid to form the DATBA.

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Goldstein, et al., "Sur l'acide dinitro-3,5-fluoro-2-benzoique", Helv. Ch Acta., v. 37, 1954, No. 134, p. 1121.
Ammon et al., "Crystallographic Studies 3,5-diamino 2-4,6-trinitrobenzamide" Acta Cryst. (1982) B38 2083.

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