4-azido-4,4-dinitro-1-butanol and derivatives thereof

Details 4-azido-4,4-dinitro-1-butanol and derivatives thereof 4-azido-4,4-dinitro-1-butanol and derivatives thereof

1987-08-05

1989-01-03

Miller, Edward A.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

204 72, 149 88, C07C11700, C06B 2500

Patent

active

047955937

ABSTRACT:
There is provided the compound 4-azido-4,4-dinitro-1-butanol (ADNBOH) and a method for making same which comprises reacting trinitromethane and acrolein at a reduced temperature to provide 4,4,4-trinitro-butyraldehyde (TNBAl), reducing the TNBSl to provide 4,4-trinitro-1-butanol (TNBOH) which is further reduced to provide 4,4-dinitro-1-butanol (DNBOH), reacting the DNBOH with acetyl chloride to provide 4,4-dinitro-1-butyl acetate (DNBAc), reacting the DNBAc with an alkali metal azide in an electrolysis cell to provide 4-azido-4,4-dinitro-1-butyl acetate (ADNBAc) and reacting the ADNBAc with a lower alcohol and recovering the 4-azido-4,4-dinitro-1-butanol (ADNBOH).
Also provided are several azidodinitro derivatives of 4-azido-4,4-dinitro-1-butanol and methods for making same.

REFERENCES:
patent: 3883377 (1975-05-01), Wright
patent: 4472311 (1984-09-01), Frankel et al.

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