3-Carboalkoxy (or phenoxy) and 3-thiocarbo-(3-chloro-2-propenyl)

Details 3-Carboalkoxy (or phenoxy) and 3-thiocarbo-(3-chloro-2-propenyl) 3-Carboalkoxy (or phenoxy) and 3-thiocarbo-(3-chloro-2-propenyl)

1976-11-11

1977-09-13

Ford, John M.

Organic compounds -- part of the class 532-570 series

Organic compounds

Four or more ring nitrogens in the bicyclo ring system

424249, C07D25710, C07D51900

Patent

active

040481662

ABSTRACT:
Compounds of the formula ##STR1## where X represents O or S and R represents C.sub.1-4 alkyl, phenyl or (C.sub.1-4 alkyl)phenyl. The compounds are prepared by reacting the ring-opened intermediate, obtained by reacting cis-1-(3-chloro-2-propenyl)-3,5,7-triaza-1-azoniatricyclo (3.3.1.1.sup.3,7) decane chloride with excess aqueous sodium hydroxide, with an equivalent amount of a corresponding halide formate or halide thioformate, ClC=X(OR), at about 0.degree. C in the presenceof a hydrogen chloride acceptor and using a non-nucleophilic organic solvent as reaction medium. The carbamate products have antimicrobial utility.

REFERENCES:
patent: 3862939 (1975-01-01), Brady
patent: 3862940 (1975-01-01), Mitchell et al.

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