2-(2-Ethoxy)ethoxyethyl benzimidazolecarbamate

Details 2-(2-Ethoxy)ethoxyethyl benzimidazolecarbamate 2-(2-Ethoxy)ethoxyethyl benzimidazolecarbamate

1975-06-20

1977-01-04

Turner, V. D.

Drug, bio-affecting and body treating compositions

Antigen, epitope, or other immunospecific immunoeffector

Parasitic organism or component thereof or substance...

2603092, A01N 922, C07D23512

Patent

active

040014231

ABSTRACT:
Phytotherapeutic compositions comprising diethylene glycol ether solutions of 2-(2-ethoxy)ethoxyethyl benzimidazolecarbamate are prepared by: (a) heating and agitating an opaque, fluid suspension of methyl 1-(butylcarbamoyl)-2-benzimidazolecarbamate and dimethylsulfoxide until the fluid clarifies whereby the butylcarbamoyl group is removed from the carbamate; (b) adding methanol to the clarified fluid to precipitate a paste containing methyl 2-benzimidazolecarbamate and methanol; (c) separating the supernatant fluid from the paste; and (d) admixing diethyleneglycol monoethyl ether with the paste to form a fluid slurry and heating the slurry, with agitation, until it clarifies to thereby obtain a diethylene glycol monoethyl ether solution of 2-(2-ethoxy)ethoxyethyl benzimidazolecarbamate, and thereafter diluting the solution with diethylene glycol monoethyl ether to obtain suitable use concentrations of the carbamate. The phytotherapeutic compositions are useful as an aid in the control of plant fungus disease.

REFERENCES:
patent: 3657443 (1972-04-01), Klopping
1 Sims et al., "Phytopathological Notes", Nov. 1969, pp. 1775-1776.

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