2-(1-hydroxycarbalkoxymethyl)-acrylonitriles and 2-(1-hydroxycar

Details 2-(1-hydroxycarbalkoxymethyl)-acrylonitriles and 2-(1-hydroxycar 2-(1-hydroxycarbalkoxymethyl)-acrylonitriles and 2-(1-hydroxycar

1985-12-03

1987-03-24

Brust, Joseph Paul

Organic compounds -- part of the class 532-570 series

Organic compounds

Nitriles

558371, 560181, C07C12130

Patent

active

046526692

ABSTRACT:
2-(1-Hydroxycarbalkoxymethyl)-acrylonitriles and 2-(1-hydroxycarbalkoxymethyl)-acrylates are prepared by a process in which an acrylonitrile or an acrylate is reacted with a glyoxylate in an aqueous medium at a pH greater than or equal to 6, in the presence of a tertiary amine as a catalyst.

REFERENCES:
patent: 3499024 (1970-03-01), Morita et al.
patent: 3743669 (1973-07-01), Hillman et al.
Garbers, et al; J. Chem. Soc., Perkin Trans. I, (1973), pp. 2016-2019.
Tetrahedron Letters, vol. 25, No. 12, pp. 1303-1306, (1984), Papageorgiou et al, Synthesis of Potentially Allergenic Chiral Alpha-(Hydroxyalkyl)Acrylates.

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