1,3-Bis-(.beta.-ethylhexyl)-5-nitro-5-methyl-hexahydropyrimidine

Details 1,3-Bis-(.beta.-ethylhexyl)-5-nitro-5-methyl-hexahydropyrimidine 1,3-Bis-(.beta.-ethylhexyl)-5-nitro-5-methyl-hexahydropyrimidine

1976-11-08

1977-09-13

Coughlan, Jr., Paul M.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D23904

Patent

active

040481697

ABSTRACT:
The process provided for the production of high-purity 1,3-bis-(.beta.-ethexyl)-5-amino-5-methyl-hexahydropyrimidine, also known as hexetidin, by reacting 1,3-bis-(.beta.-ethylhexyl)-5-nitro-5-methyl-hexahydropyrimidine with naphthalene-1,5-disulphonic acid in a solvent to selectively precipitate the novel intermediate compound 1,3-bis-(.beta.-ethylhexyl)-5-nitro-5-methyl-hexahydropyrimidine-naphthale ne-1,5-disulphonate, which is separated off, treated with aqueous alkali to produce 1,3-bis-(.beta.-ethylhexyl)-5-nitro-5-methyl-hexahydropyrimidine, and subsequently hydrogenated to produce high-purity hexetidin.

REFERENCES:
patent: 3749721 (1973-07-01), Herrmann et al.
Senkus, J. Amer. Chem. Soc., vol. 68 (1946) pp. 1611-1613.

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