1,1'-bis(3-aminopropyl)-2,2'-diimidazole

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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C07D40304

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053997050

ABSTRACT:
1,1'-bis(3-aminopropyl)-2,2'-diimidazole of the formula I ##STR1## is prepared by a novel process in which 2,2'-diimidazole of the formula II ##STR2## is reacted with acrylonitrile of the formula III ##STR3## in the presence of basic catalysts at from 80.degree. to 150.degree. C., and hydrogenation is carried out with excess hydrogen in the presence of ammonia on catalysts which contain cobalt, nickel, ruthenium and/or noble metals at from 40.degree. to 200.degree. C. under from 10 to 200 bar.

REFERENCES:
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Yamauchi et al. II, "Reactivity of 2,4(5)-dialkylimidazoles, etc" CA 85:177382g (1976).
Sawa et al, "Synthesis of imidazole compounds, etc" CA 71:101773a (1969).
Houben-Weyl, vol. 11/1, pp. 545-569 (1955).
Organic Syntheses 27 (1947) pp. 18-20.
Organic Reactions 5 (1942) pp. 79-135.
Melloni et al. Arzneim. Forschung 25 (1975) pp. 9-14.

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