1,1,1-trichloro-2-nitroethane production

Details 1,1,1-trichloro-2-nitroethane production 1,1,1-trichloro-2-nitroethane production

1992-07-06

1994-11-15

Rotman, Alan L.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

568924, 544336, 546304, 546329, 548193, 564395, C07C20502, C07C20106

Patent

active

053649893

ABSTRACT:
Methods for the production of 1,1,1-trihalogeno-2-nitroethanes from 1,1-dihalogenoethylene by using nitric acid or its salt and hydrogen chloride or hydrogen bromide or its salt, and for the production of .alpha.-unsaturated amines from the 1,1,1-trihalogeno-2-nitroethanes which are useful as insecticides.

REFERENCES:
patent: 4518812 (1985-05-01), Baasner et al.
patent: 4533776 (1985-08-01), Baasner et al.
Derwent Publications Ltd. J6 2048-681-A Abstract.
Chemical Abstracts, vol. 64, 1966, p. 8023.
Chemical Abstracts, vol. 53, 1959, p. 1111.
J. Org. Chem., vol. 25, Bachman et al., "Nitration Studies XII. Nitrohalogenation of Negatively Substituted Olefins with Mixtures of Dinitorgen Tetroxide and Halogens", 1960, pp. 1312-1323.
William A. Pryor, "Free Radicals" (McGraw-Hill Book Company, 1966), Halogenation by Bromine, pp. 189-190.
Buehler & Pearson, "Survey of Organic Synthesis", (1970, Wiley-Interscience, New York, London, Sydney, Toronto), pp. 357-358.
Isnikawa, "Synthesis and Function of Fluorine Compounds", pp. 15, 34, 35, 155, 156, 177, and English translation thereof, 1987 CMC Co. Tokyo.
Merck Index, Eleventh Edition, 1989, Nos. 4720, 4721 and 4723, pp. 759-760.

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