Automatic preparation of sample for analysis

Chemistry: physical processes – Physical processes – Crystallization

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23253R, 23259, 177114, 426231, G01G 1324, G01N 3300, G01N 3302

Patent

active

040836908

ABSTRACT:
A novel automatic apparatus for preparing a sample for analysis and a novel method for preparation of the sample are provided, whereby specified fractions of plural liquid samples can be automatically and successively collected by distillation. The apparatus comprises an inert gas charging means, a multi-way selector liquid sampler means operated by a timer, a liquid sample charging and discharging means operated by a timer, a distillation still, a fraction selector means and fraction receivers, which are connected in that order by pipe lines. The apparatus and method are especially useful, for example, for preparing a sample for analysis of a diacetyl-odor component and a sample for Kjeldahl determination method.

REFERENCES:
patent: 3028225 (1962-04-01), Sheen
patent: 3236321 (1966-02-01), Katagiri et al.
patent: 3515672 (1970-06-01), Reinish et al.
patent: 3826621 (1974-07-01), Johnson, Jr. et al.
patent: 3846075 (1974-11-01), Cioffi
patent: 3964869 (1976-06-01), Aegidius
West et al., Studies on Diacetyl in Beer, American Society of Brewing Chemists, Proceedings, pp. 81-88 (1952).
Owades et al., Microdetermination of Diacetyl in Beer, American Society of Brewing Chemists, Proceedings, pp. 22-25 (1963).

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