Process for the preparation of squaric acid by the electrolysis

Chemistry: electrical and wave energy – Processes and products

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C07B 2906

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active

044616813

ABSTRACT:
An improved process for the preparation of squaric acid, its complexes and/or salts, by means of a process for the electrolytic cathodic reductive tetramerization of carbon monoxide, involving the usage of an anhydrous aliphatic nitrile solvent containing from 3 to about 8 carbon atoms.

REFERENCES:
patent: 3833489 (1974-09-01), Ercoli et al.
Silvestri et al., Gazzetta Chimica Italiana, vol. 102, pp. 818-821, (1972).
Silvestri et al., Electrochimica Acta, vol. 23, pp. 413-417, (1978).

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