Reagent for the quantitative determination of water and its use

Chemistry: physical processes – Physical processes – Crystallization

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23230HC, 252408, G01N 3318

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active

043559980

ABSTRACT:
A reagent for the quantitative determination of water, used together with an iodine-containing titrating solution, the reagent containing sulfur dioxide and an anhydrous alkali metal trimethyl acetate or a mixture of anhydrous alkali metal trimethyl acetate and an anhydrous alkali metal salicylate dissolved in 2-methoxy ethanol, methanol or in a mixture of 2-methoxy ethanol and methanol in a volume ratio of at least 10 to 90. This reagent is distinguished in that the increase of the blind value is minimized even at elevated temperatures.

REFERENCES:
patent: 3656907 (1972-04-01), Delmonte
Verhoef et al., Analytica Chimica Acta, vol. 94, 1977, pp. 395-403.
Anon., Chemisch Weekblad Magazine, Mar. 1979, p. 135.

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