Process for preparing triazolethiols

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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260308C, C07D24904

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active

040948811

ABSTRACT:
1,2,3-Triazole-4(5)-thiol is prepared by treating 1-benzyl-1,2,3-triazole with a strong base, treating the resulting anion with sulfur, removing the benzyl group by reductive means, and acidifying the resulting thiolate with strong acid.

REFERENCES:
patent: 3867380 (1975-02-01), Dunn et al.
Goerdeler et al., Ber. Dent. Chem., vol. 99, pp. 1618-1631 (1966).
Begtrup, Chem. Abstracts, vol. 76, Abstract No. 72454t (1972).
Dunn et al., Chem. Abstracts, vol. 84, Abstract No. 159507b (1976).

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