Process for preparing stereospecific nerolidol and ester thereof

Details Process for preparing stereospecific nerolidol and ester thereof Process for preparing stereospecific nerolidol and ester thereof

1977-03-17

1978-08-08

Gerstl, Robert

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

C07C 2924

Patent

active

041057007

ABSTRACT:
A process for obtaining a stereospecific nerolidol at the .DELTA..sup.6 -position thereof by rectifying a mixture of .DELTA..sup.6 -cis-nerolidol and .DELTA..sup.6 -trans-nerolidol in rectification column having from 10 to 100 theoretical plates with a reflux ratio of from 2 to 200 at a temperature below 230.degree. C. under reduced pressure to separate each stereospecific nerolidol from said mixture.

REFERENCES:
patent: 1644546 (1927-10-01), Ruzicka
patent: 1999110 (1935-04-01), Ruzicka
patent: 2848502 (1958-08-01), Surmatis
patent: 3296080 (1967-01-01), Meuly et al.
patent: 3755469 (1973-08-01), Pasedach et al.
Bates, J. Org. Chem., vol. 28, pp. 1086-1089 (1963).
Eliel, Stereochemistry of Carbonyl Compounds, pp. 326-346 (1962).

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