Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing
Patent
1979-08-01
1980-12-30
Lone, Werren B.
Organic compounds -- part of the class 532-570 series
Organic compounds
Oxygen containing
568806, C07C 3906
Patent
active
042425280
ABSTRACT:
A novel process for producing isopropenyl phenol such as p-isopropenyl phenol which comprises continuously feeding oligomers of isopropenyl phenol having a degree of polymerization of 2 to 5 into a high-boiling inert organic reaction medium such as an alkylnaphthalene heated at 150.degree. to 250.degree. C. under a pressure of 10 to 100 mmHg while maintaining the concentration of the oligomers in the reaction medium at not more than 30% by weight, thereby thermally decomposing the oligomers in the reaction medium; and continuously distilling off the resulting isopropenyl phenol out of the reaction system and recovering it. The process almost quantitatively gives isopropenyl phenol having reduced contents of impurities.
REFERENCES:
patent: 1798813 (1931-03-01), Schoeller et al.
patent: 4054611 (1977-10-01), Mimaki et al.
patent: 4131749 (1978-12-01), Kiedik et al.
Derwent Belgium Patent Report Belgian 593, 367, vol. 74A, Mar. 30, 1961, p. C11.
Hattori Minoru
Kato Nobukatu
Morimoto Yoshio
Takase Tsutomu
Yuasa Teruo
Lone Werren B.
Mitsui Toatsu Chemicals Incorporated
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