Process for preparing isopropenyl phenol

Organic compounds -- part of the class 532-570 series – Organic compounds – Oxygen containing

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568806, C07C 3906

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042425280

ABSTRACT:
A novel process for producing isopropenyl phenol such as p-isopropenyl phenol which comprises continuously feeding oligomers of isopropenyl phenol having a degree of polymerization of 2 to 5 into a high-boiling inert organic reaction medium such as an alkylnaphthalene heated at 150.degree. to 250.degree. C. under a pressure of 10 to 100 mmHg while maintaining the concentration of the oligomers in the reaction medium at not more than 30% by weight, thereby thermally decomposing the oligomers in the reaction medium; and continuously distilling off the resulting isopropenyl phenol out of the reaction system and recovering it. The process almost quantitatively gives isopropenyl phenol having reduced contents of impurities.

REFERENCES:
patent: 1798813 (1931-03-01), Schoeller et al.
patent: 4054611 (1977-10-01), Mimaki et al.
patent: 4131749 (1978-12-01), Kiedik et al.
Derwent Belgium Patent Report Belgian 593, 367, vol. 74A, Mar. 30, 1961, p. C11.

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