Method of preparing 1,1,1-azidodinitro compounds

Details Method of preparing 1,1,1-azidodinitro compounds Method of preparing 1,1,1-azidodinitro compounds

1982-07-22

1984-09-18

Brust, Joseph Paul

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

149 88, C06B 2500, C07C11700

Patent

active

044723113

ABSTRACT:
1,1,1-azidodinitro compounds such as 1,1,1-azidodinitroethane are prepared by reacting the corresponding 1,1,1-trinitromethyl compound with lithium azide in the presence of a dipolar aprotic solvent. 1,1,1-azidodinitro compounds are also known as 1-azido-1,1-dinitro compounds.

REFERENCES:
patent: 3157683 (1964-11-01), Feuer et al.
patent: 3317595 (1967-05-01), Paciorek
patent: 3883377 (1975-05-01), Wright
Fieser, et al., "Reagents for Organic Synthesis", vol. 6, (1977), p. 327; John Wiley & Sons, N.Y.
C.A., 75, (1971), 98106k, Margoretha, et al.
C.A., 82, (1975), 139404w, Henrick, et al.

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