Process for the separation of alcohols by distillation

Organic compounds -- part of the class 532-570 series – Organic compounds – Carbohydrates or derivatives

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536124, 536127, 203 89, 203 91, 159 49, 159DIG10, 159DIG16, O07H 1504

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057102619

ABSTRACT:
Aliphatic alcohols with up to 30 and especially with 6 to 18 carbon atoms are separated from a mixture of alkyl glycosides and alcohols which are unreacted during the production of these glycosides, by single or multi-stage distillation. The alcohols are distilled off by a drop film evaporator to impoverish the reaction mixture to residual alcohol contents of 5 wt % and under. The strip load of the drop film evaporator is set to at least 1.0 m.sup.3 /h m, especially at least 1.8 m.sup.3 /h m and preferably at least 3.0 m.sup.3 /h m. It is possible to reduce the alcohol content of the product to any value between 0.1 and 5 wt % at acceptable overall cost.

REFERENCES:
patent: 4611055 (1986-09-01), Yamamoto et al.
patent: 5079350 (1992-01-01), Fujita et al.
patent: 5138046 (1992-08-01), Wuest et al.
patent: 5234554 (1993-08-01), Muller et al.
patent: 5304639 (1994-04-01), Gibson

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