Production of acid orthophosphoric acid ester mixtures

Chemistry of carbon compounds – Dipeptides – e.g. – aspartame – anserine – carnosine – etc.

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260980, C07F 909

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active

041419383

ABSTRACT:
Orthophosphoric acid esters are made by reacting phosphorus(V)-oxide with an alcoholic component. More specifically, phosphorus(V)-oxide is reacted by mixing or kneading it with a blend consisting of a monohydric alcohol and an alkane polyol containing 2 to 12 carbon atoms and 2 to 6 hydroxyl groups, at approximately 0 to 120.degree. C. with the exclusion of moisture, in the presence of an inert gas, and over a period of approximately 1 to 6 hours. The resulting reaction product is cooled.

REFERENCES:
patent: 2510033 (1950-05-01), Kyrides
patent: 3276916 (1966-10-01), Wurstner
patent: 3407150 (1968-10-01), Wismer et al.

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