Step-wise supercritical extraction of carbonaceous residua

Mineral oils: processes and products – Fractionation – Liquid extraction with solvents

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208309, 208313, 208314, 208952, C10G 104

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active

046751017

ABSTRACT:
A method of fractionating a mixture containing high boiling carbonaceous material and normally solid mineral matter includes processing with a plurality of different supercritical solvents. The mixture is treated with a first solvent of high critical temperature and solvent capacity to extract a large fraction as solute. The solute is released as liquid from solvent and successively treated with other supercritical solvents of different critical values to extract fractions of differing properties. Fractionation can be supplemented by solute reflux over a temperature gradient, pressure let down in steps and extractions at varying temperature and pressure values.

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