Purification of (hydrocarbylthio) aromatic amines

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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564430, 564440, 546293, 548484, 548541, 568 38, 568 57, C07C 8526

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active

047271914

ABSTRACT:
A (hydrocarbylthio)aromatic amine, such as a methylthiosubstituted toluenediamine, is separated from corresponding aromatic amines containing fewer hydrocarbylthio groups by washing an organic solution of the amine mixture with a dilute aqueous acid having a pKa value below 7 to extract at least a portion of the corresponding aromatic amines.

REFERENCES:
patent: 3228989 (1966-01-01), Reifschneider
patent: 3763239 (1973-10-01), Smolin
patent: 3931321 (1976-01-01), Planker et al.
patent: 4594453 (1986-06-01), Ranken et al.

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