Process for introducing three substituents in cyanuric chloride

Organic compounds -- part of the class 532-570 series – Organic compounds – Four or more ring nitrogens in the bicyclo ring system

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544197, 544208, 544210, 544211, 544213, 544219, 544113, 544212, 544209, 544198, C07D25146, C07D25152, C07D25166, C07D25170

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042811236

ABSTRACT:
Three substituents are introduced into cyanuric acid in the presence of an acid binding agent by working in a manner permitting high mixing and therefore high reaction velocities and permitting high throughputs in small tubular containers by introducing liquid cyanuric chloride through a nozzle in the upper portion of the mixing apparatus in countercurrent flow to upwardly flowing reactants (and acid binding agent) introduced from at least one lower nozzle above a breast shaped constriction in the lower, open portion of the apparatus. The process can be carried out at normal, reduced or elevated pressure.

REFERENCES:
patent: 3925377 (1975-12-01), Geiger et al.
Ullmann, Enzyklopadie der Technischen Chemie, 3rd Edition, 1954, vol. 1, pp. 743-744 and 769-770.

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