Formation of particulate polypyrrolidone

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – From carboxylic acid or derivative thereof

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528312, 528319, 528326, C08G 6924

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active

042811058

ABSTRACT:
A process for polymerizing 2-pyrrolidone to form a particulate material suitable for melt extrusion processes is disclosed. The process involves agitating to form particles at a critical point during the polymerization in which a friable gel exists. The gel is formed as a result of the addition of polymerization accelerators to the polymerization mixture but as the accelerated polymerization proceeds the gel soon hardens to a tough cake which can no longer be broken up by agitation. If the polymerizing mixture is agitated before the formation of the gel only very fine particles are formed.

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