Method for the production of reinforced composites

Plastic and nonmetallic article shaping or treating: processes – Including step of generating heat by friction

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264 56, 264 86, 264 87, 501 95, C04B 3328

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048407631

ABSTRACT:
A process for the production of reinforced refractory composite structures which may be of high density and shaped in desired three dimensional configurations. The shaped composite structures are produced by forming a suspension of particulate materials including a colloidal refractory power, colloidal sintering aid, and refractory reinforcement whiskers in a carrier liquid. The colloidal suspension is conformed to a desired configuration and brought into contact with a semipermeable membrane. A pressure is imposed on the suspension in the desired configuration to expel liquid from the suspension through the membrane to arrive at a green composite having a density of at least 40% of theoretical density. After drying, the green composite is then sintered under conditions to form an intergranular liquid phase in the composite providing further densification. A specific composite is a silicon carbide reinforced silicon nitride composite. The green composite may be sintered to provide a density of at least 93% of theoretical to produce a closed impermeable composite surface. The composite may then be subjected to hot isostatic pressing.

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German, R. M., "Liquid Phase Sintering," 1985 Plenum Press, New York, p. 224.

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