Process for preparing 3,4-dicyano-1,2,5-thiadiazole

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07D28510

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040628604

ABSTRACT:
3,4-DICYANO-1,2,5-THIADIAZOLE IS PREPARED BY REACTING DIAMINOMALEONITRILE (DAMN) with thionyl chloride (SOCl.sub.2) at a temperature of 40.degree. C. up to the boiling point of thionyl chloride wherein the molar ratio of SOCl.sub.2 /DAMN is between 2:1 and 10:1.

REFERENCES:
shew, Ph.D. Dissertation, 1959, Indiana University, pp. 11-13, 16 & 62.

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