Production of anhydrous ethanol

Distillation: processes – separatory – Distilling to separate or remove only water – From organic compound

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203 23, 203 25, 203 27, 203 68, 203 69, 203 75, 203 77, 203 78, 203DIG13, B01D 336

Patent

active

043728227

ABSTRACT:
Substantially anhydrous, i.e., absolute, ethanol is distilled at high thermal efficiency from a dilute feedstock such as a fermentate ("beer") containing one or more low boiling components whose removal at least in part prior to anhydrous distillation is necessary in order to achieve an acceptable degree of phase separation in a decanter. Most of the low boiling component(s) are removed from the feed in a rectifying column with the balance of the low boiling component(s), insufficient in amount to seriously interfere with proper operation of the decanter, being removed from the system employing a light-ends column. Both the anhydrous column and the light-ends column are operated at substantially superatmospheric pressure with thermal values recovered from these columns being used in the operation of the rectifying column.

REFERENCES:
patent: 3445345 (1969-05-01), Katzen et al.
patent: 4161429 (1979-07-01), Baiel et al.

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