Process for the preparation of 2-[N-(2-hydroxyethyl)-N-lower alk

Details Process for the preparation of 2-[N-(2-hydroxyethyl)-N-lower alk Process for the preparation of 2-[N-(2-hydroxyethyl)-N-lower alk

1979-03-05

1980-06-17

Hines, Robert V.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260558R, 260559D, C07C 8512

Patent

active

042083494

ABSTRACT:
Process for the production of 2-[N-(2-hydroxyethyl)-N-lower alkylaminomethyl]benzhydrols by reducing N-(2-haloethyl)-N-lower alkyl-o-benzoylbenzamides in an inert solvent with sodium borohydride in the presence of an alkanoic acid.

REFERENCES:
patent: 3830803 (1974-08-01), Klohs et al.
patent: 3978085 (1976-08-01), Eberlin
patent: 4071557 (1978-01-01), Mattner et al.
patent: 4083871 (1978-04-01), Houlihan et al.
Ventron Alembic, "Reduction of Amides with Sodium Borohydride", pp. 6-7.
Umino et al., "Tetrahedron Letters", No. 10, pp. 763-766.
Maki et al., "Chemistry & Industry", Apr. 13, 1976, pp. 322-323.

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